C₆₆H₉₄N₄O₁₂SSi₃

Base Information

Chemical Name:C₆₆H₉₄N₄O₁₂SSi₃
CAS No.:1334176-56-5
Molecular Formula:C₆₆H₉₄N₄O₁₂SSi₃
Molecular Weight:1251.81
Hs Code.:

C<sub>66</sub>H<sub>94</sub>N<sub>4</sub>O<sub>12</sub>SSi<sub>3</sub>

Synonyms:C₆₆H₉₄N₄O₁₂SSi₃

Suppliers and Price of C₆₆H₉₄N₄O₁₂SSi₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₆H₉₄N₄O₁₂SSi₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₆H₉₄N₄O₁₂SSi₃

There total 11 articles about C₆₆H₉₄N₄O₁₂SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1334176-55-4
C₆₄H₉₀N₄O₁₂Si₃

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 1334176-56-5
C₆₆H₉₄N₄O₁₂SSi₃

Guidance literature:: With acetic anhydride; acetic acid; at 20 ℃; for 50h; Inert atmosphere;
DOI:10.1002/chem.201101821

Reference yield:

: 1334176-53-2
N⁽³⁾-benzyloxymethyl-3',5'-O-di(triethylsilyl)-5,6-dihydrothymidine

: 1334176-56-5
C₆₆H₉₄N₄O₁₂SSi₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: pyridine hydrogenfluoride / acetonitrile / 4 h / -20 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 0 - 20 °C / Inert atmosphere

4.1: acetic anhydride; acetic acid / 50 h / 20 °C / Inert atmosphere

With 1H-imidazole; acetic anhydride; pyridine hydrogenfluoride; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201101821

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1334176-56-5
C₆₆H₉₄N₄O₁₂SSi₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: pyridine hydrogenfluoride / acetonitrile / 4 h / -20 °C / Inert atmosphere

6.1: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 0 - 20 °C / Inert atmosphere

7.1: acetic anhydride; acetic acid / 50 h / 20 °C / Inert atmosphere

With 1H-imidazole; N-Bromosuccinimide; acetic anhydride; pyridine hydrogenfluoride; acetic acid; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201101821