β-elemene acetate

Base Information

Chemical Name:β-elemene acetate
CAS No.:1162008-48-1
Molecular Formula:C₁₇H₂₆O₂
Molecular Weight:262.392
Hs Code.:

Synonyms:β-elemene acetate

Suppliers and Price of β-elemene acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-elemene acetate

Chemical Property:

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Technology Process of β-elemene acetate

There total 3 articles about β-elemene acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 885691-35-0
monochloro β-elemene

: 127-09-3
sodium acetate

: 1162008-48-1
β-elemene acetate

Guidance literature:: In N,N-dimethyl-formamide;
DOI:10.1016/j.biopha.2018.07.107

Reference yield:

: 515-13-9
β-elemene

: 127-09-3
sodium acetate

: 1162008-48-1
β-elemene acetate

: C₁₇H₂₆O₂

Guidance literature:: β-elemene; With sodium hypochlorite; acetic acid; In dichloromethane; at 0 - 5 ℃; for 6h;

sodium acetate; In N,N-dimethyl-formamide; at 120 ℃; for 8h; Overall yield = 75 %;
DOI:10.1021/acsmedchemlett.7b00035

Reference yield:

: 515-13-9
β-elemene

: 1162008-48-1
β-elemene acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hypochlorite / acetic acid / 6 h / 0 - 20 °C

2: potassium iodide / dichloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide / 12 h / 95 °C

With sodium hypochlorite; potassium iodide; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; acetic acid;
DOI:10.1007/s00044-013-0615-3