2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

Base Information

Chemical Name:2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene
CAS No.:82464-08-2
Molecular Formula:C₂₇H₂₁NO₈
Molecular Weight:487.466
Hs Code.:

Synonyms:2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

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Chemical Property of 2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

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Technology Process of 2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

There total 3 articles about 2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 82464-05-9
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-1,4-dihydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

: 82464-08-2
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

Guidance literature:: With tert.-butylhydroperoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 84h; Ambient temperature;
DOI:10.1248/cpb.30.569

Reference yield:

: 67258-01-9,82534-85-8
4b,10bβ,11,12-tetrahydro-4bβ,12β-(N-phenylepoxyimino)oxychelerythrine

: 82464-08-2
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / H₂ / 10percent Pd-C / methanol / 0.25 h / Ambient temperature

3: 69 percent / tert-butyl hydroperoxide, DBU / benzene / 84 h / Ambient temperature

With tert.-butylhydroperoxide; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium on activated charcoal; In methanol; benzene;
DOI:10.1248/cpb.30.569

Reference yield:

: 82464-01-5
trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone

: 82464-08-2
2-3',4'-dimethoxy-2'-methoxycarbonylphenyl-2,3-epoxy-1,2,3,4-tetrahydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

Guidance literature:: Multi-step reaction with 2 steps

2: 69 percent / tert-butyl hydroperoxide, DBU / benzene / 84 h / Ambient temperature

With tert.-butylhydroperoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene;
DOI:10.1248/cpb.30.569