<α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Base Information

Chemical Name:<α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle
CAS No.:122082-70-6
Molecular Formula:C₂₆H₃₃NO₅
Molecular Weight:439.552
Hs Code.:

Synonyms:<α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

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Chemical Property of <α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

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Technology Process of <α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

There total 4 articles about <α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 122082-67-1
(α-amino p-methoxy benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

: 122082-70-6
<α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: With sodium; In water; at 0 - 20 ℃; for 40h;
DOI:10.1016/0223-5234(88)90091-8

Reference yield:

: 57078-08-7,57129-25-6,61490-75-3,93781-25-0,116696-95-8,116696-96-9,145415-55-0,145415-56-1,82801-37-4
acide cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique

: 122082-70-6
<α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether

2: 77 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

3: 47 percent / Al/Hg, 5percent HgCl / ethanol; H₂O / 2 h

4: 97 percent / Na / H₂O / 40 h / 0 - 20 °C

With pyridine; aluminum amalgam; hydroxylamine hydrochloride; sodium; mercury(II) chloride; In diethyl ether; ethanol; water;
DOI:10.1016/0223-5234(88)90091-8

Reference yield:

: 93740-32-0,93740-33-1,122082-22-8
ester methylique de l'acide cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique

: 122082-70-6
<α-(N-benzyloxycarbonyl amino) p-methoxy benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

2: 47 percent / Al/Hg, 5percent HgCl / ethanol; H₂O / 2 h

3: 97 percent / Na / H₂O / 40 h / 0 - 20 °C

With pyridine; aluminum amalgam; hydroxylamine hydrochloride; sodium; mercury(II) chloride; In ethanol; water;
DOI:10.1016/0223-5234(88)90091-8