trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester
CAS No.:865241-63-0
Molecular Formula:C₂₅H₂₅F₉O₄S
Molecular Weight:592.523
Hs Code.:

trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester

Synonyms:trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester

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Chemical Property of trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester

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Technology Process of trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester

There total 8 articles about trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 865238-33-1
trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-methoxymethoxy-3-trifluoromethyl-1-butenyl)phenyl]propyl}-2-methylphenyl ester

: 865241-63-0
trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1016/j.bmc.2013.01.042

Reference yield:

: 865235-89-8
trifluoromethanesulfonic acid 4-[1-ethyl-1-(4-hydroxy-3-methylphenyl)-propyl]-2-methylphenyl ester

: 865241-63-0
trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 18 h / 110 °C

1.2: pH 7

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C

3.2: 0.5 h / 0 °C

4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 1 h / 0 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 1 h / 20 - 60 °C

6.1: pyridine / dichloromethane / 0.5 h / 0 °C

7.1: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C

With pyridine; n-butyllithium; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; trifluoroacetic acid; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 55041-27-5
3,3-bis[4-hydroxy-3-methylphenyl]pentane

: 865241-63-0
trifluoromethanesulfonic acid 4-{1-ethyl-1-[3-methyl-4-((E)-4,4,4-trifluoro-3-hydroxy-3-trifluoromethyl-1-butenyl)phenyl] propyl}-2-methylphenyl ester

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine / dichloromethane / 1 h / 0 °C

2.1: triethylamine / copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 18 h / 110 °C

2.2: pH 7

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C

4.2: 0.5 h / 0 °C

5.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 1 h / 0 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

6.2: 1 h / 20 - 60 °C

7.1: pyridine / dichloromethane / 0.5 h / 0 °C

8.1: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C

With pyridine; n-butyllithium; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; trifluoroacetic acid; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;