2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite

Base Information

• Chemical Name: 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite
• CAS No.: 80032-43-5
• Molecular Formula: C₁₁H₁₃F₁₂NO₂S
• Molecular Weight: 451.277
• Mol file: 80032-43-5.mol

Synonyms:2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite

Chemical Property of 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite

There total 5 articles about 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.1%

C25H19F36NO3S (80032-16-2) → 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol (335-99-9) + 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite (80032-43-5)

Guidance literature:

In diethyl ether; water; at 0 ℃; for 1h;

Reference yield:

C11H13F14NOS (80027-81-2) → diethylamidosulfurous fluoride (1550-61-4) + 1,1,2,2,3,3,4,4,5,5,6,6,7-tridecafluoroheptane (2708-11-4) + 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite (80032-43-5) + bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)diethylaminofluorosulfurane (80027-88-9)

Guidance literature:

under 0.05 - 0.08 Torr; Further byproducts given; the bath temperature gradually raised to 90 deg C;

Reference yield:

C11H13F14NOS (80027-81-2) → diethylamino-sulfur trifluoride (38078-09-0) + 1,1,2,2,3,3,4,4,5,5,6,6,7-tridecafluoroheptane (2708-11-4) + 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite (80032-43-5) + bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)diethylaminofluorosulfurane (80027-88-9)

Guidance literature:

under 0.05 - 0.08 Torr; Further byproducts given; the bath temperature gradually raised to 90 deg C;

upstream raw materials:

C₁₁H₁₃F₁₄NOS

C₂₅H₁₉F₃₆NO₃S