16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one

Base Information

Chemical Name:16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one
CAS No.:1334215-34-7
Molecular Formula:C₂₈H₃₈N₄O
Molecular Weight:446.636
Hs Code.:

Synonyms:16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one

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Chemical Property of 16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one

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Technology Process of 16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one

There total 4 articles about 16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1334215-13-2
16β-(1H-1,2,3-triazol-1-yl)-5α-androstan-3,17-dione

: 100-61-8
N-methylaniline

: 1334215-34-7
16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 40 ℃; for 24h; pH=Ca. 6;
DOI:10.1016/j.ejmech.2011.05.030

Reference yield:

: 28507-02-0
16α-bromo-3β-hydroxy-5α-androstan-17-one

: 1334215-34-7
16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent / acetone / 0 °C

2: acetonitrile / 24 h / 80 °C

3: sodium cyanoborohydride; acetic acid / methanol / 24 h / 40 °C / pH Ca_. 6

With Jones reagent; sodium cyanoborohydride; acetic acid; In methanol; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2011.05.030

Reference yield:

: 481-29-8
Epiandrosterone

: 1334215-34-7
16β-(1H-1,2,3-triazol-1-yl)-3β-(N-methylphenylamino)-5α-androstan-17-one

Guidance literature:: Multi-step reaction with 4 steps

1: copper(ll) bromide / methanol / 12 h / 65 °C

2: Jones reagent / acetone / 0 °C

3: acetonitrile / 24 h / 80 °C

4: sodium cyanoborohydride; acetic acid / methanol / 24 h / 40 °C / pH Ca_. 6

With Jones reagent; sodium cyanoborohydride; acetic acid; copper(ll) bromide; In methanol; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2011.05.030