2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene

Base Information

• Chemical Name: 2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene
• CAS No.: 188844-81-7
• Molecular Formula: C₃₀H₃₂N₂O₂
• Molecular Weight: 452.596

Synonyms:2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene

Chemical Property of 2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene

Chemical Property:

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Technology Process of 2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene

There total 6 articles about 2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-{2-[methyl(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphtalen-2-yl)amino]-phenyl}-terephthalamic acid methyl ester (188844-78-2) → 2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene (188844-81-7)

Guidance literature:

With PPA; In dichloromethane; at 110 ℃; for 24h;

Reference yield:

N-methyl-N-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphtalen-2-yl)-1,2-phenylenediamine (188844-76-0) + Monomethyl terephthalate (1679-64-7) → 2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene (188844-81-7)

Guidance literature:

With trichlorophosphate; In toluene; at 80 ℃; for 96h;

Reference yield:

2-[amido-4-benzoic acid methyl-ester]-1-methyl-amino[1,2,3,4-tetrahydro-1,1,4,4-tetramethyl-naphthalene]-benzene → 2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene (188844-81-7)

Guidance literature:

With polyphosphoric acid; at 110 ℃; for 18h;

upstream raw materials:

N-methyl-N-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphtalen-2-yl)-1,2-phenylenediamine

Monomethyl terephthalate

N-{2-[methyl(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphtalen-2-yl)amino]-phenyl}-terephthalamic acid methyl ester

Downstream raw materials:

4-(5,7,7,10,10-pentamethyl-7,8,9,10,12,13-hexahydro-5H-5,13-diaza-benzo[4,5]cyclohepta[1,2-b]naphthalen-12-yl)-benzoic acid methyl ester

4-(2-bromo-5,7,7,10,10-pentamethyl-7,8,9,10-tetrahydro-5H-5,13-diazabenzo[4,5]cyclohepta[1,2-b]naphthalen-12-yl)benzoic acid methyl ester

methyl 4-(5H-2,3-(2,5-dimethyl-2,5-hexano)-5-methyl-8-nitrodibenzo[b,e][1,4]diazepin-11-yl)benzoate

4-(5,7,7,10,10,13-hexamethyl-7,8,9,10,12,13-hexahydro-5H-5,13-diaza-benzo[4,5]cyclohepta[1,2-b]naphthalen-12-yl)-benzoic acid methyl ester

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