methyl 4-(5H-8-amino-2,3-(2,5-dimethyl-2,5-hexano)-5-methyldibenzo[b,e][1,4]diazepin-11-yl)benzoate

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Chemical Name:methyl 4-(5H-8-amino-2,3-(2,5-dimethyl-2,5-hexano)-5-methyldibenzo[b,e][1,4]diazepin-11-yl)benzoate
CAS No.:951211-99-7
Molecular Formula:C₃₀H₃₃N₃O₂
Molecular Weight:467.611
Hs Code.:

Synonyms:methyl 4-(5H-8-amino-2,3-(2,5-dimethyl-2,5-hexano)-5-methyldibenzo[b,e][1,4]diazepin-11-yl)benzoate

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Chemical Property of methyl 4-(5H-8-amino-2,3-(2,5-dimethyl-2,5-hexano)-5-methyldibenzo[b,e][1,4]diazepin-11-yl)benzoate

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Technology Process of methyl 4-(5H-8-amino-2,3-(2,5-dimethyl-2,5-hexano)-5-methyldibenzo[b,e][1,4]diazepin-11-yl)benzoate

There total 2 articles about methyl 4-(5H-8-amino-2,3-(2,5-dimethyl-2,5-hexano)-5-methyldibenzo[b,e][1,4]diazepin-11-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 188845-12-7
methyl 4-(5H-2,3-(2,5-dimethyl-2,5-hexano)-5-methyl-8-nitrodibenzo[b,e][1,4]diazepin-11-yl)benzoate

: 951211-99-7
methyl 4-(5H-8-amino-2,3-(2,5-dimethyl-2,5-hexano)-5-methyldibenzo[b,e][1,4]diazepin-11-yl)benzoate

Guidance literature:: With hydrogenchloride; iron; In ethanol; for 2h;
DOI:10.1248/cpb.47.1778

Reference yield:

: 188844-81-7
2-[amido-4-benzoic acid methyl ester]-1-methylamino[1,2,3,4-tetrahydro-1,1,4,4-tetramethylnaphthalene]-4-nitrobenzene

: 951211-99-7
methyl 4-(5H-8-amino-2,3-(2,5-dimethyl-2,5-hexano)-5-methyldibenzo[b,e][1,4]diazepin-11-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 45.5 percent / KNO₃; H₂SO₄ / 2.5 h / 0 °C

2: 100 percent / Fe; aq. HCl / ethanol / 2 h

With hydrogenchloride; sulfuric acid; iron; potassium nitrate; In ethanol; 1: Nitration / 2: Reduction;
DOI:10.1248/cpb.47.1778