tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium

Base Information

Chemical Name:tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium
CAS No.:12213-09-1
Molecular Formula:C₂₆H₂₀O₃PV
Molecular Weight:462.358
Hs Code.:

Synonyms:tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium

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Chemical Property of tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium

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Technology Process of tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium

There total 5 articles about tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.8%

: tetracarbonyl(η(5)-cyclopentadienyl)vanadium(I)

: 12213-09-1
tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium

Guidance literature:: With triphenylphosphine; In benzene; Irradiation (UV/VIS); evapn. at reduced pressure and in high vac.;

Reference yield: 65.0%

: 89184-67-8
((C₅H₅)V(C₆H₅)P(C₆H₅)2)

: 201230-82-2
carbon monoxide

: 12213-09-1
tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium

Guidance literature:: In tetrahydrofuran; reaction of CpV(C6H5)P(C6H5)2 with CO at room temp. (Ar); evapn. of the reaction soln. to dryness and dissolving the residue in toluene, pptn. of red brown crystals on cooling to -78°C, filtering off the crystals and drying (oil pump vacuum), elem. anal.;

Reference yield: 3.0%

: tetracarbonyl(η(5)-cyclopentadienyl)vanadium(I)

: 603-35-0
triphenylphosphine

: C₅H₅V(CO)2(P(C₆H₅)3)2

: 12213-09-1
tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium

Guidance literature:: In benzene; byproducts: CO; Irradiation (UV/VIS); 1 h photolysis; concn. by evapn., chromy. on alumina, evapn., recrystn. from chloroform/hexane, washing with hexane, drying;
DOI:10.1021/ic50205a042