methyl 3-O-benzyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate

Base Information

Chemical Name:methyl 3-O-benzyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate
CAS No.:1227467-76-6
Molecular Formula:C₂₆H₄₄O₈Si₂
Molecular Weight:540.802
Hs Code.:

Synonyms:methyl 3-O-benzyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-benzyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate

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Technology Process of methyl 3-O-benzyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate

There total 1 articles about methyl 3-O-benzyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 87326-77-0,87326-78-1
methyl 3-O-benzyl-L-idopyranosyluronate

: 1227467-76-6
methyl 3-O-benzyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate

Guidance literature:: With 1H-imidazole; In acetonitrile; at -45 ℃; for 41h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2010.03.077

Reference yield: 68.0%

: 1227467-76-6
methyl 3-O-benzyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate

: 123-76-2
levulinic acid

: 1227467-77-7
methyl 3-O-benzyl-4-O-levulinyl-1,2-O-(1,1,3,3-tetraisopropyldisiloxanylidene)-α-L-idopyranuronate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2010.03.077