2-Hydroxydimedon

Base Information

• Chemical Name: 2-Hydroxydimedon
• CAS No.: 83538-02-7
• Molecular Formula: C₈H₁₂O₃
• Molecular Weight: 156.181
• Mol file: 83538-02-7.mol

Synonyms:2-Hydroxydimedon

Chemical Property of 2-Hydroxydimedon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Hydroxydimedon

There total 3 articles about 2-Hydroxydimedon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

dimedone (126-81-8) → 2-chloro-5,5-dimethyl-1,3-cyclohexanedione (7298-89-7) + 2-Hydroxydimedon (83538-02-7)

Guidance literature:

With 1H-imidazole; citrate-phosphate buffer; Mn-meso-tetrakis(3,5-disulphonatomesityl)porphyrinato; polyvinylpyridinium polymer (MnTMPS/PVP); dihydrogen peroxide; sodium chloride; In water; acetonitrile; for 1h; Product distribution; Ambient temperature; other reaction partner systems;

DOI:10.1039/c39900001414

Reference yield:

diazodimedone (1807-68-7) → 2-Hydroxydimedon (83538-02-7)

Guidance literature:

With sulfuric acid; copper;

Reference yield:

2-Amino-3-hydroxy-5,5-dimethyl-cyclohex-2-enone (32583-63-4) → 2-Hydroxydimedon (83538-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous HCl; NaNO₂

2: aqueous H₂SO₄; copper

With hydrogenchloride; sulfuric acid; copper; sodium nitrite;

upstream raw materials:

diazodimedone

dimedone

2-Amino-3-hydroxy-5,5-dimethyl-cyclohex-2-enone

Downstream raw materials:

3-anilino-2-hydroxy-5,5-dimethyl-cyclohex-2-enone

5-Hydroxy-5-(1-hydroxy-4,4-dimethyl-2,6-dioxocyclohexyl)-2,2-dimethyl-1,3-dioxan-4,6-dion