DIAZODIMEDONE

Base Information

• Chemical Name: DIAZODIMEDONE
• CAS No.: 1807-68-7
• Molecular Formula: C8H10 N2 O2
• Molecular Weight: 166.18
• Hs Code.: 2927000090
• Mol file: 1807-68-7.mol

Synonyms:2-Diazo-5,5-dimethyl-1,3-cyclohexanedione;2-Diazodimedone; 3,5-Dioxo-4-diazo-1,1-dimethylcyclohexane; Diazodimedone; NSC601821

Chemical Property of DIAZODIMEDONE

Chemical Property:

• Melting Point: 105-108 °C
• PSA: 71.53000
• LogP: 0.69646

Purity/Quality:

97% ^*data from raw suppliers

Diazodimedone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIAZODIMEDONE

There total 7 articles about DIAZODIMEDONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

dimedone (126-81-8) → diazodimedone (1807-68-7)

Guidance literature:

With dmap; [bmim]Br; Methanesulfonyl azide; at 25 ℃; for 1h;

DOI:10.1016/j.tetlet.2008.02.159

Reference yield: 80.0%

dimedone (126-81-8) + (Azidochlormethylen)dimethylammoniumchlorid → diazodimedone (1807-68-7)

Guidance literature:

In dichloromethane; for 4h; Heating;

Reference yield: 71.0%

4-nitrophenyl azide (1516-60-5) + dimedone (126-81-8) → diazodimedone (1807-68-7) + 6,6-dimethyl 1-(4-nitrophenyl)-6,7-dihydro-1H-benzo[d][1,2,3]triazol-4(5H)-one (24706-55-6)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; at 55 ℃; for 120h;

upstream raw materials:

2-amino-5,5-dimethylcyclohexane-1,3-dione

2-Amino-3-hydroxy-5,5-dimethyl-cyclohex-2-enone

dimedone

4-nitrophenyl azide

Downstream raw materials:

methyl 4,4-dimethyl-2-oxocyclopentanecarboxylate

1.1.1'.1'-Tetramethyl-4.4'-azo-dicyclohexandion-(3.5)

6,6-dimethyl-3-phenyl-2-phenylimino-2,3,6,7-tetrahydro-5H-cyclopenta[e][1,3]oxazin-4-one

4,4-Dimethyl-2-oxocyclopentancarbonsaeure-p-bromanilid

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