1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride

Base Information

• Chemical Name: 1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride
• CAS No.: 1104938-03-5
• Molecular Formula: C₁₅H₂₁ClN₂O*ClH
• Molecular Weight: 317.258

Synonyms:1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride

Chemical Property of 1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride

Chemical Property:

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Technology Process of 1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride

There total 1 articles about 1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-hydroxy-ethyl)-piperidine-4-carboxylic acid benzylamide (1104938-01-3) → 1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride (1104938-03-5)

Guidance literature:

With thionyl chloride; In toluene; at 20 - 30 ℃;

Reference yield:

1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride (1104938-03-5) + aniline (62-53-3) → 1-(2-phenylamino-ethyl)-piperidine-4-carboxylic acid benzylamide (1104938-05-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; sodium iodide; In acetonitrile; at 100 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

meta-fluoroaniline (372-19-0) + 1-(2-chloro-ethyl)-piperidine-4-carboxylic acid benzylamide hydrochloride (1104938-03-5) → 1-[2-(3-fluoro-phenylamino)-ethyl]-piperidine-4-carboxylic acid benzyl amide (1104938-07-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; sodium iodide; In acetonitrile; at 100 ℃; for 0.166667h; Microwave irradiation;

upstream raw materials:

1-(2-hydroxy-ethyl)-piperidine-4-carboxylic acid benzylamide

Downstream raw materials:

1-(2-phenylamino-ethyl)-piperidine-4-carboxylic acid benzylamide

1-[2-(3-fluoro-phenylamino)-ethyl]-piperidine-4-carboxylic acid benzyl amide

1-[2-(4-methanesulfonyl-phenylamino)-ethyl]-piperidine-4-carboxylic acid benzylamide

1-[2-(3,5-difluoro-phenylamino)-ethyl]-piperidine-4-carboxylic acid benzylamide

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