N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide
CAS No.:1322645-03-3
Molecular Formula:C₂₀H₃₅N₃O₂S
Molecular Weight:381.583
Hs Code.:

Synonyms:N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide

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Chemical Property of N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide

There total 6 articles about N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1322645-01-1
N-phthaloyl-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine

: 1322645-03-3
N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide

Guidance literature:: With hydrazine hydrate; In ethanol; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.jmedchem.5b01832

Reference yield:

: 56125-49-6
N-(3-aminopropyl)-p-toluenesulfonamide

: 1322645-03-3
N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene / 12 h / Inert atmosphere; Reflux

2.1: sodium tetrahydroborate / ethanol / 12 h / 20 °C / Inert atmosphere

3.1: sodium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux

4.1: hydrazine hydrate / ethanol / 3 h / Inert atmosphere; Reflux

4.2: 1.5 h / Inert atmosphere

With sodium tetrahydroborate; sodium carbonate; hydrazine hydrate; In ethanol; toluene; acetonitrile;
DOI:10.1021/jm2002603

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1322645-03-3
N-(3-((3-aminopropyl)(cyclohexylmethyl)amino)propyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene / 20 °C / Inert atmosphere

2.1: water / methanol / 6 h / 4 °C / Inert atmosphere

3.1: toluene / 12 h / Inert atmosphere; Reflux

4.1: sodium tetrahydroborate / ethanol / 12 h / 20 °C / Inert atmosphere

5.1: sodium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux

6.1: hydrazine hydrate / ethanol / 3 h / Inert atmosphere; Reflux

6.2: 1.5 h / Inert atmosphere

With sodium tetrahydroborate; water; sodium carbonate; hydrazine hydrate; In methanol; ethanol; toluene; acetonitrile;
DOI:10.1021/jm2002603