benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate

Base Information

• Chemical Name: benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate
• CAS No.: 886981-12-0
• Molecular Formula: C₂₀H₁₈N₆O₃
• Molecular Weight: 390.401

Synonyms:benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate

Chemical Property of benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate

Chemical Property:

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Technology Process of benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate

There total 1 articles about benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2,3-Benzotriazole (95-14-7,27556-51-0) + N-[(benzyloxy)carbonyl]-L-histidine (14997-58-1) → benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate (886981-12-0)

Guidance literature:

1,2,3-Benzotriazole; With thionyl chloride; In tetrahydrofuran; at 20 ℃; for 0.333333h;

N-[(benzyloxy)carbonyl]-L-histidine; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1055/s-2006-926287

Reference yield: 96.0%

pyrrolidine (123-75-1) + benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate (886981-12-0) → benzyl N-[(1S)-1-(1H-imidazol-4-ylmethyl)-2-oxo-2-(1-pyrrolidinyl)ethyl]carbamate (35048-62-5)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1055/s-2006-926287

Reference yield: 96.0%

benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-(1H-imidazol-4-ylmethyl)-2-oxoethyl]carbamate (886981-12-0) + (R)-1-phenyl-ethyl-amine (3886-69-9) → benzyl N-((1S)-1-(1H-imidazol-4-ylmethyl)-2-oxo-2-{[(1R)-1-phenylethyl]amino}ethyl)carbamate

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1055/s-2006-926287

upstream raw materials:

1,2,3-Benzotriazole

N-[(benzyloxy)carbonyl]-L-histidine

Downstream raw materials:

benzyl N-[(1S)-1-(1H-imidazol-4-ylmethyl)-2-oxo-2-(1-pyrrolidinyl)ethyl]carbamate

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