methyl 2,3-di-O-(4-methoxybenzyl)-5-O-(tert-butyldiphenylsilyl)-α-D-arabinofuranoside

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Chemical Name:methyl 2,3-di-O-(4-methoxybenzyl)-5-O-(tert-butyldiphenylsilyl)-α-D-arabinofuranoside
CAS No.:1186016-52-3
Molecular Formula:C₃₈H₄₆O₇Si
Molecular Weight:642.865
Hs Code.:

Synonyms:methyl 2,3-di-O-(4-methoxybenzyl)-5-O-(tert-butyldiphenylsilyl)-α-D-arabinofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3-di-O-(4-methoxybenzyl)-5-O-(tert-butyldiphenylsilyl)-α-D-arabinofuranoside

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Technology Process of methyl 2,3-di-O-(4-methoxybenzyl)-5-O-(tert-butyldiphenylsilyl)-α-D-arabinofuranoside

There total 2 articles about methyl 2,3-di-O-(4-methoxybenzyl)-5-O-(tert-butyldiphenylsilyl)-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 824-94-2
p-methoxybenzyl chloride

: (2R,3S,4S,5S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-3,4-diol

: 1186016-52-3
methyl 2,3-di-O-(4-methoxybenzyl)-5-O-(tert-butyldiphenylsilyl)-α-D-arabinofuranoside

Guidance literature:: With tetrabutylammomium bromide; sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 12h;

Reference yield:

: 56607-40-0
methyl D-arabinofuranoside

: 1186016-52-3
methyl 2,3-di-O-(4-methoxybenzyl)-5-O-(tert-butyldiphenylsilyl)-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / 3 h / 20 °C

2: tetrabutylammomium bromide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 0 - 20 °C

With 1H-imidazole; tetrabutylammomium bromide; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.3998/ark.5550190.0014.222