[Ni(chloride)2(2-methoxy-5-sulphamoyl-N-((1-ethylpyrrolidin-2-yl)methyl)benzamide)2(water)2]*(water)

Base Information

• Chemical Name: [Ni(chloride)2(2-methoxy-5-sulphamoyl-N-((1-ethylpyrrolidin-2-yl)methyl)benzamide)2(water)2]*(water)
• CAS No.: 1235753-75-9
• Molecular Formula: C₃₀H₅₀Cl₂N₆NiO₁₀S₂*H₂O
• Molecular Weight: 866.504
• Mol file: 1235753-75-9.mol

Synonyms:[Ni(chloride)2(2-methoxy-5-sulphamoyl-N-((1-ethylpyrrolidin-2-yl)methyl)benzamide)2(water)2]*(water)

Chemical Property of [Ni(chloride)2(2-methoxy-5-sulphamoyl-N-((1-ethylpyrrolidin-2-yl)methyl)benzamide)2(water)2]*(water)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Ni(chloride)2(2-methoxy-5-sulphamoyl-N-((1-ethylpyrrolidin-2-yl)methyl)benzamide)2(water)2]*(water)

There total 1 articles about [Ni(chloride)2(2-methoxy-5-sulphamoyl-N-((1-ethylpyrrolidin-2-yl)methyl)benzamide)2(water)2]*(water) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

nickel(II) chloride hexahydrate + N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-methoxy-5-sulfamoylbenzamide (15676-16-1) → [Ni(chloride)2(2-methoxy-5-sulphamoyl-N-((1-ethylpyrrolidin-2-yl)methyl)benzamide)2(water)2]*(water) (1235753-75-9)

Guidance literature:

In ethanol; water; addn. of hot (60°C) soln. of Cl compd. in ethanol/water (1:1) to hot (60°C) soln. of C compd. in ethanol/water (1:1), stirring under reflux for 2 h; filtration, washing with ethanol/water (1:1) and diethyl ether, elem. anal.;

DOI:10.1016/j.saa.2010.03.016

Reference yield:

[Ni(chloride)2(2-methoxy-5-sulphamoyl-N-((1-ethylpyrrolidin-2-yl)methyl)benzamide)2(water)2]*(water) (1235753-75-9) → nickel(II) oxide (1313-99-1)

Guidance literature:

In neat (no solvent, solid phase); byproducts: H2O, Cl2, H2NSO2C6H3(OCH3)C(O)NHCH2(C4H7N)C2H5; (N2); heating S compd. (10°C/min), 40-900°C; not isolated;

DOI:10.1016/j.saa.2010.03.016

upstream raw materials:

N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-methoxy-5-sulfamoylbenzamide

Downstream raw materials:

nickel(II) oxide