N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide]

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Chemical Name:N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide]
CAS No.:191986-40-0
Molecular Formula:C₃₉H₆₀N₄O₁₀S₂
Molecular Weight:809.058
Hs Code.:

Synonyms:N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide]

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Chemical Property of N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide]

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Technology Process of N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide]

There total 1 articles about N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77429-97-1
N¹,N⁵-ditosyl-3-azapentane-1,5-diamine

: 191986-40-0
N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide]

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / benzene / 120 h / Heating

2: 66 percent / K₂CO₃, Cs₂CO₃, NaI / acetonitrile / 19 h / Heating

With potassium carbonate; caesium carbonate; sodium iodide; In acetonitrile; benzene;
DOI:10.1002/hlca.19970800314

Reference yield: 97.0%

: 191986-40-0
N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide]

: 191986-41-1
N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis{N-[2-(2-hyroxyethoxy)ethyl]4-methylbenzenesulfonamide}

Guidance literature:: With toluene-4-sulfonic acid; In methanol; for 12h; Ambient temperature;
DOI:10.1002/hlca.19970800314

Reference yield:

: 191986-40-0
N,N'-{[(2-cyanoethyl)imino]di(ethane-2,1-diyl)}bis[4-methyl-N-(2-{2-[(tetrahydro-2H-pyran-2-yl)oxy]-ethoxy}ethyl)benzenesulfonamide]

: 117539-09-0
3-[4,10,16,19,22-Pentakis-(toluene-4-sulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaaza-cyclotetracos-7-yl]-propionitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / toluene-4-sulfonic acid monohydrate / methanol / 12 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 1.) 0 deg C, 2 h, 2.) RT, 2 h

3: 50 percent / Cs₂CO₃ / dimethylformamide / 51 h / 100 °C

With caesium carbonate; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19970800314