1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

Base Information

Chemical Name:1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole
CAS No.:1392809-42-5
Molecular Formula:C₂₈H₂₁ClN₆O₃S
Molecular Weight:557.032
Hs Code.:

Synonyms:1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

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Chemical Property of 1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

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Technology Process of 1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

There total 4 articles about 1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1392809-41-4
3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

: 2888-06-4
3-chlorophenylsulfonyl chloride

: 1392809-42-5
1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

Guidance literature:: 3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.333333h;

3-chlorophenylsulfonyl chloride; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 851199-66-1
1-(4-methoxybenzyl)-5-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1H-tetrazole

: 1392809-42-5
1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / Inert atmosphere; Reflux

2.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C

2.2: 2 h / 20 °C

With potassium tert-butylate; di(n-butyl)tin oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; 1.1: Suzuki- Miyaura reaction;

Reference yield:

: 5-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1H-tetrazole

: 1392809-42-5
1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 12 h / 40 °C

2.1: di(n-butyl)tin oxide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / Inert atmosphere; Reflux

3.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C

3.2: 2 h / 20 °C

With potassium tert-butylate; di(n-butyl)tin oxide; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; acetonitrile; 2.1: Suzuki- Miyaura reaction;