3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole

Base Information

Chemical Name:3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole
CAS No.:1392809-31-2
Molecular Formula:C₂₀H₁₃ClN₆O₂S
Molecular Weight:436.881
Hs Code.:

Synonyms:3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole

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Chemical Property of 3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole

Chemical Property:

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Technology Process of 3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole

There total 5 articles about 3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1392809-42-5
1-(3-chlorophenylsulfonyl)-3-(4-(1-(4-methoxybenzyl)-1H-tetrazol-5-yl)phenyl)-1H-indazole

: 1392809-31-2
3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 48h;

Reference yield:

: 5-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1H-tetrazole

: 1392809-31-2
3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 12 h / 40 °C

2.1: di(n-butyl)tin oxide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / Inert atmosphere; Reflux

3.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C

3.2: 2 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 48 h / 20 °C

With potassium tert-butylate; di(n-butyl)tin oxide; potassium carbonate; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; acetonitrile; 2.1: Suzuki- Miyaura reaction;

Reference yield:

: 171364-82-2
4-cyanophenylboronic acid pinacol ester

: 1392809-31-2
3-(4-(1H-tetrazol-5-yl)phenyl)-1-(3-chlorophenylsulfonyl)-1H-indazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: di(n-butyl)tin oxide / 1,2-dimethoxyethane / 0.33 h / 20 - 150 °C / Microwave irradiation

2.1: potassium carbonate / acetonitrile / 12 h / 40 °C

3.1: di(n-butyl)tin oxide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / Inert atmosphere; Reflux

4.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / 20 °C

4.2: 2 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 48 h / 20 °C

With potassium tert-butylate; di(n-butyl)tin oxide; potassium carbonate; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; acetonitrile; 3.1: Suzuki- Miyaura reaction;