2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine

Base Information

• Chemical Name: 2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine
• CAS No.: 1245751-32-9
• Molecular Formula: C₂₆H₃₉NO₄Si
• Molecular Weight: 457.685

Synonyms:2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine

Chemical Property of 2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine

Chemical Property:

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Technology Process of 2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine

There total 2 articles about 2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

2-[1,3]dioxolan-2-yl-6-iodo-4-methyl-3-(2-trimethylsilanylethoxymethoxy)-pyridine (1245751-27-2) + tributyl-[3-(3-methyl-butyl)phenyl]stannane (1245751-12-5) → 2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine (1245751-32-9)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; cesium fluoride; In N,N-dimethyl-formamide; at 50 ℃;

DOI:10.1002/chem.201000315

Reference yield: 44.0%

1-bromo-3-(3-methyl-butyl)-benzene (1245751-10-3) + 2-[1,3]dioxolan-2-yl-4-methyl-6-tributylstannanyl-3-(2-trimethylsilanylethoxymethoxy)-pyridine (1245751-30-7) → 2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine (1245751-32-9)

Guidance literature:

With copper(l) iodide; tri-tert-butyl phosphine; cesium fluoride; palladium dichloride; In N,N-dimethyl-formamide; at 50 ℃;

DOI:10.1002/chem.201000315

Reference yield: 92.0%

2-[1,3]dioxolan-2-yl-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-3-(2-trimethylsilanylethoxymethoxy)-pyridine (1245751-32-9) → 3-hydroxy-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-pyridine-2-carbaldehyde (1245751-34-1)

Guidance literature:

With cerium(III) chloride heptahydrate; sodium iodide; In acetonitrile; at 45 ℃; for 32h;

DOI:10.1002/chem.201000315

upstream raw materials:

2-[1,3]dioxolan-2-yl-6-iodo-4-methyl-3-(2-trimethylsilanylethoxymethoxy)-pyridine

tributyl-[3-(3-methyl-butyl)phenyl]stannane

1-bromo-3-(3-methyl-butyl)-benzene

2-[1,3]dioxolan-2-yl-4-methyl-6-tributylstannanyl-3-(2-trimethylsilanylethoxymethoxy)-pyridine

Downstream raw materials:

3-hydroxy-4-methyl-6-[3-(3-methyl-butyl)-phenyl]-pyridine-2-carbaldehyde

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