ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate

Base Information

Chemical Name:ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate
CAS No.:1431881-22-9
Molecular Formula:C₂₅H₁₈FNO₃S₂
Molecular Weight:463.553
Hs Code.:

Synonyms:ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate

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Chemical Property of ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate

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Technology Process of ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate

There total 3 articles about ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 56442-17-2
4-((4-fluorobenzyl)oxy)benzaldehyde

: 1431881-49-0
ethyl 3H-thieno[3',2':3,4]benzo[1,2-d][1,2,3]dithiazole-7-carboxylate 2-oxide

: 1431881-22-9
ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate

Guidance literature:: With piperidine; In dimethyl sulfoxide; at 20 - 120 ℃;
DOI:10.1016/j.tet.2013.04.001

Reference yield:

: 7-(ethoxycarbonyl)thieno[3′,2′:3,4]benzo[1,2-d][1,2,3]dithiazol-2-ium chloride

: 1431881-22-9
ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: water

2: piperidine / dimethyl sulfoxide / 20 - 120 °C

With piperidine; water; In dimethyl sulfoxide;
DOI:10.1016/j.tet.2013.04.001

Reference yield:

: 25785-10-8
ethyl 5-amino-1-benzothiophene-2-carboxylate

: 1431881-22-9
ehyl 2-(4-((4-fluorobenzyl)oxy)phenyl)thieno[3',2':3,4]-benzo-[1,2-d]thiazole-7-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; disulfur dichloride / 2 h / 0 - 40 °C

2: water

3: piperidine / dimethyl sulfoxide / 20 - 120 °C

With piperidine; disulfur dichloride; water; acetic acid; In dimethyl sulfoxide; 1: |Herz Benzothiazole Synthesis;
DOI:10.1016/j.tet.2013.04.001