C₂₈H₄₂N₈O₃

Base Information

Chemical Name:C₂₈H₄₂N₈O₃
CAS No.:1440509-94-3
Molecular Formula:C₂₈H₄₂N₈O₃
Molecular Weight:538.693
Hs Code.:

C<sub>28</sub>H<sub>42</sub>N<sub>8</sub>O<sub>3</sub>

Synonyms:C₂₈H₄₂N₈O₃

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Chemical Property of C₂₈H₄₂N₈O₃

Chemical Property:

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Technology Process of C₂₈H₄₂N₈O₃

There total 21 articles about C₂₈H₄₂N₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₃₄H₅₀N₈O₃

: 1440509-94-3
C₂₈H₄₂N₈O₃

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; for 12h;
DOI:10.1039/c3md00021d

Reference yield:

: 1440509-97-6
C₁₇H₂₃N₅O₃

: 1440509-94-3
C₂₈H₄₂N₈O₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2.1: hydrazine hydrate / ethanol / 2 h / Reflux

3.1: sodium cyanoborohydride; acetic acid / methanol / 0 °C

4.1: methanol / 72 h / Reflux

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / -15 - 20 °C

5.2: 2 h / 0 °C

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran

7.1: hydrazine / ethanol / 80 °C

8.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C

9.1: hydrogenchloride / methanol; 1,4-dioxane / 12 h

With hydrogenchloride; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; sodium cyanoborohydride; hydrazine hydrate; acetic acid; triethylamine; triphenylphosphine; hydrazine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane;
DOI:10.1039/c3md00021d

Reference yield:

: 111005-65-3
(-)-2,3-(cyclohexylidenedioxy)-4-cyclopentenone

: 1440509-94-3
C₂₈H₄₂N₈O₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: copper(I) bromide dimethylsulfide complex / tetrahydrofuran / 0.25 h / -78 °C

1.2: 5 h / -78 °C

2.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 1 h / -15 - 20 °C

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 72 h / 0 - 20 °C

4.1: ozone / dichloromethane / -78 °C

4.2: 1 h / -78 - 20 °C / Inert atmosphere

4.3: 1 h / 0 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

7.1: hydrazine hydrate / ethanol / 2 h / Reflux

8.1: sodium cyanoborohydride; acetic acid / methanol / 0 °C

9.1: methanol / 72 h / Reflux

10.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / -15 - 20 °C

10.2: 2 h / 0 °C

11.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran

12.1: hydrazine / ethanol / 80 °C

13.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C

14.1: hydrogenchloride / methanol; 1,4-dioxane / 12 h

With hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; copper(I) bromide dimethylsulfide complex; cerium(III) chloride heptahydrate; di-isopropyl azodicarboxylate; sodium cyanoborohydride; ozone; hydrazine hydrate; acetic acid; triethylamine; triphenylphosphine; trifluoroacetic acid; hydrazine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane;
DOI:10.1039/c3md00021d