Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester

Base Information

Chemical Name:Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester
CAS No.:196938-76-8
Molecular Formula:C₂₃H₃₃N₃O₈
Molecular Weight:479.53
Hs Code.:

Synonyms:Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester

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Chemical Property of Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester

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Technology Process of Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester

There total 7 articles about Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35793-73-8
N-(tert-butyloxycarbonyl)-γ-benzyl-D-glutamic acid

: 196938-76-8
Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / diethyl ether / 0.5 h / 0 °C

2: 100 percent / H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

3: 4-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C

4: 4-methylmorpholine / dimethylformamide; tetrahydrofuran / 0.42 h / Ambient temperature

5: 90 percent / HCl / ethyl acetate / 1.5 h / Ambient temperature

6: 4-methylmorpholine / tetrahydrofuran; dimethylformamide / 0.5 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 110473-10-4
N-Boc-D-Glu α-methyl ester

: 196938-76-8
Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

2: 4-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C

3: 4-methylmorpholine / dimethylformamide; tetrahydrofuran / 0.42 h / Ambient temperature

4: 90 percent / HCl / ethyl acetate / 1.5 h / Ambient temperature

5: 4-methylmorpholine / tetrahydrofuran; dimethylformamide / 0.5 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 3303-84-2
3-(tert-butyloxycarbonylamino)propionic acid

: 196938-76-8
Benzyl N-(tert-butoxycarbonyl)-β-alanyl-(α-methyl (2R)-glutamyl)-γ-glycinate ester

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C

2: 4-methylmorpholine / tetrahydrofuran; dimethylformamide / 0.5 h / Ambient temperature

With 4-methyl-morpholine; In tetrahydrofuran; N,N-dimethyl-formamide;