Technology Process of C34H29NO3
There total 4 articles about C34H29NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylsilane; trifluoroacetic acid;
In
dichloromethane;
at 0 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: aluminum (III) chloride / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere
1.2: 0 °C
2.1: pyrrolidine / methanol / 0.5 h / 20 °C / Inert atmosphere
2.2: 16 h / Reflux
3.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere
4.1: trifluoroacetic acid; triethylsilane / dichloromethane / 0.5 h / 0 °C
With
pyrrolidine; methanol; triethylsilane; aluminum (III) chloride; sodium tetrahydroborate; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate; methanol / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere
2: trifluoroacetic acid; triethylsilane / dichloromethane / 0.5 h / 0 °C
With
methanol; triethylsilane; sodium tetrahydroborate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;