5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one

Base Information

Chemical Name:5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one
CAS No.:1373243-15-2
Molecular Formula:C₃₀H₂₃NO₄
Molecular Weight:461.517
Hs Code.:

Synonyms:5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one

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Chemical Property of 5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one

Chemical Property:

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Technology Process of 5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one

There total 1 articles about 5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1221748-96-4
1'-(diphenylmethyl)-6-hydroxyspiro[1-benzofuran-3,3'-indol]-2'(1'H)-one

: 75-36-5
acetyl chloride

: 1373243-15-2
5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one

Guidance literature:: 1'-(diphenylmethyl)-6-hydroxyspiro[1-benzofuran-3,3'-indol]-2'(1'H)-one; acetyl chloride; With aluminum (III) chloride; In dichloromethane; at 0 - 20 ℃; for 48h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; at 0 ℃;

Reference yield: 90.0%

: 1373243-15-2
5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one

: 107-30-2
chloromethyl methyl ether

: 1373243-36-7
5-acetyl-1'-benzhydryl-6-(methoxymethoxy)-2H-spiro[benzofuran-3,3'-indolin]-2'-one

Guidance literature:: 5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.25h;

chloromethyl methyl ether; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 3h;

Reference yield: 54.0%

: 1191-95-3
cyclobutanone

: 1373243-15-2
5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one

: 1373243-16-3
C₃₄H₂₇NO₄

Guidance literature:: 5-acetyl-1'-benzhydryl-6-hydroxy-2H-spiro[benzofuran-3,3'-indolin]-2'-one; With pyrrolidine; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;

cyclobutanone; In methanol; for 16h; Reflux;