acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester

Base Information

Chemical Name:acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester
CAS No.:503025-63-6
Molecular Formula:C₃₀H₄₂O₄
Molecular Weight:466.661
Hs Code.:

Synonyms:acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester

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Chemical Property of acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester

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Technology Process of acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester

There total 12 articles about acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 503025-62-5
8-(4-methoxyphenyl)-3-methylene-7-octyloxy-8-phenyloctan-2-one

: 503025-63-6
acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester

Guidance literature:: With bis-trimethylsilanyl peroxide; tin(IV) chloride; rac-diaminocyclohexane; In dichloromethane; at 20 ℃; for 40h;
DOI:10.1021/ja029139v

Reference yield:

: 503025-52-3
tert-butyldimethyl-[3-(3-phenyloxiranyl)propoxy]silane

: 503025-63-6
acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: 71 percent / CuI / tetrahydrofuran / 6 h / 20 °C

2.1: 40 percent / sodium hydride / dimethylformamide / 5 h / 20 °C

3.1: 89 percent / acetic acid / tetrahydrofuran; H₂O

4.1: methanesulfonyl chloride; triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

4.2: 92 percent / NaI / acetone / 1.5 h / Heating

5.1: 56 percent / potassium carbonate / acetone / 22 h / Heating

6.1: 58 percent / formaldehyde; K₂CO₃ / dioxane; H₂O / 12 h / 35 °C

7.1: 71 percent / trans-1,2-(diamino)cyclohexane; SnCl₄; bis(trimethylsilyl)peroxide / CH₂Cl₂ / 40 h / 20 °C

With formaldehyd; bis-trimethylsilanyl peroxide; tin(IV) chloride; sodium hydride; potassium carbonate; acetic acid; rac-diaminocyclohexane; methanesulfonyl chloride; triethylamine; copper(l) iodide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja029139v

Reference yield:

: 591-50-4
iodobenzene

: 503025-63-6
acetic acid 6-(4-methoxyphenyl)-1-methylene-5-octyloxy-6-phenylhexyl ester

Guidance literature:: Multi-step reaction with 11 steps

1.1: diisopropylamine / Pd(PPh₃)4 / tetrahydrofuran / 0.33 h / 20 °C

1.2: 99 percent / CuI / tetrahydrofuran / 12 h

2.1: 99 percent / LAH / tetrahydrofuran / 20 h / Heating

3.1: 95 percent / imidazole / dimethylformamide / 0 - 20 °C

4.1: 72 percent / m-CPBA; NaOAc / CH₂Cl₂ / 6 h / 20 °C

5.1: 71 percent / CuI / tetrahydrofuran / 6 h / 20 °C

6.1: 40 percent / sodium hydride / dimethylformamide / 5 h / 20 °C

7.1: 89 percent / acetic acid / tetrahydrofuran; H₂O

8.1: methanesulfonyl chloride; triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

8.2: 92 percent / NaI / acetone / 1.5 h / Heating

9.1: 56 percent / potassium carbonate / acetone / 22 h / Heating

10.1: 58 percent / formaldehyde; K₂CO₃ / dioxane; H₂O / 12 h / 35 °C

11.1: 71 percent / trans-1,2-(diamino)cyclohexane; SnCl₄; bis(trimethylsilyl)peroxide / CH₂Cl₂ / 40 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; formaldehyd; bis-trimethylsilanyl peroxide; sodium acetate; tin(IV) chloride; sodium hydride; potassium carbonate; acetic acid; rac-diaminocyclohexane; methanesulfonyl chloride; triethylamine; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja029139v