bromo [η⁵-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II)

Base Information

• Chemical Name: bromo [η⁵-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II)
• CAS No.: 669772-09-2
• Molecular Formula: C₃₇H₂₀Br₆O₂Ru
• Molecular Weight: 1077.06

Synonyms:bromo [η⁵-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II)

Chemical Property of bromo [η⁵-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II)

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Technology Process of bromo [η⁵-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II)

There total 1 articles about bromo [η⁵-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

dodecacarbonyl-triangulo-triruthenium (15243-33-1) + 1-bromo-1,2,3,4,5-penta(4-bromophenyl)cyclopentadiene (669772-05-8) → bromo [η5-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II) (669772-09-2)

Guidance literature:

In toluene; under Ar; reflux 3 equiv. of 1-bromo-1,2,3,4,5-penta(p-bromophenyl)cyclopentadiene with soln. of Ru3(CO)12 in toluene; chromy. (SiO2/cyclohexane-CH2Cl2 40 %);

DOI:10.1039/b307577j

Reference yield: 83.0%

bromo [η5-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II) (669772-09-2) + sodium iodide (7681-82-5,24359-64-6,41927-88-2,115813-40-6) → iodo [η5-1,2,3,4,5-pentakis-(p-iodophenyl)cyclopentadienyldicarbonyl]ruthenium(II)

Guidance literature:

With copper(l) iodide; trans-N,N'-dimethylcyclohexane-1,2-diamine; In 1,4-dioxane; at 110 ℃; for 36h; Schlenk technique; Inert atmosphere; Darkness;

DOI:10.1002/chem.201903615

Reference yield: 82.0%

bromo [η5-1,2,3,4,5-pentakis(p-bromophenyl)cyclopentadienyl dicarbonyl]ruthenium(II) (669772-09-2) + thallium hydrotris{6-[(ethylsulfanyl)methyl]indazol-1-yl}borate → C65H54BBr5N6RuS3

Guidance literature:

In acetonitrile; at 100 ℃; for 0.5h; Microwave irradiation; Sealed tube;

DOI:10.1002/ejoc.201800990

upstream raw materials:

dodecacarbonyl-triangulo-triruthenium

1-bromo-1,2,3,4,5-penta(4-bromophenyl)cyclopentadiene

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