4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose

Base Information

Chemical Name:4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose
CAS No.:501012-23-3
Molecular Formula:C₂₆H₃₄O₁₀S
Molecular Weight:538.616
Hs Code.:

Synonyms:4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose

Suppliers and Price of 4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose

There total 2 articles about 4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 124-63-0
methanesulfonyl chloride

: 225233-48-7
4-C-hydroxymethyl-1,2-O-isopropylidene-3,5-di-O-p-methoxybenzyl-α-D-ribo-pentofuranose

: 501012-23-3
4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose

Guidance literature:: With pyridine; at 20 ℃;

Reference yield: 89.0%

: 501012-23-3
4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose

Guidance literature:

Reference yield:

: 501012-23-3
4-C-methanesulfonyloxymethyl-3,5-di-O-(p-methoxybenzyl)-1,2-O-isopropylidene-α-D-ribofuranose

: 501012-33-5
(1S,3S,4R,7S)-3-(4-fluoro-3-methylphenyl)-7-(p-methoxybenzyloxy)-1-(p-methoxybenzyloxymethyl)-2,5-dioxabicyclo[2.2.1]heptane

Guidance literature:: Multi-step reaction with 5 steps

1: aq. HCl / 72 h / 20 °C

2: NaH / dimethylformamide; various solvent(s) / 12 h / 20 °C

3: 82 percent / aq. AcOH / 4 h / 50 °C

4: 85 percent / tetrahydrofuran / 12 h / 0 °C

5: 84 percent / TMAD; tributylphosphine / benzene / 12 h / 20 °C

With hydrogenchloride; tributylphosphine; diamide; sodium hydride; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; benzene; 4: Grignard reaction;