Technology Process of C47H85NO6
There total 11 articles about C47H85NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 5h;
Inert atmosphere;
DOI:10.1002/anie.201006035
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dmap / tetrahydrofuran / 12 h / 20 °C
2: sodium azide; 15-crown-5 / N,N-dimethyl-formamide / 48 h / 70 °C / Inert atmosphere
3: methanol; sodium methylate / tetrahydrofuran / 0.5 h / 20 °C
4: Pd(OH)2 (10% on C); hydrogen / ethanol; acetic acid / 2 h / 20 °C
5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 20 °C / Inert atmosphere
With
methanol; dmap; sodium azide; 15-crown-5; Pd(OH)2 (10% on C); hydrogen; sodium methylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/anie.201006035
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 6 h / 20 °C
2: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 0 - 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 20 °C / Inert atmosphere
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydrogencarbonate; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/anie.201006035