(9,9-dimethyl-2-tosyl-2,3,9,9a-tetrahydro-1H-indeno[2,1-c]pyridin-4-yl)(phenyl)methanone

Base Information

Chemical Name:(9,9-dimethyl-2-tosyl-2,3,9,9a-tetrahydro-1H-indeno[2,1-c]pyridin-4-yl)(phenyl)methanone
CAS No.:1542560-52-0
Molecular Formula:C₂₈H₂₇NO₃S
Molecular Weight:457.593
Hs Code.:

Synonyms:(9,9-dimethyl-2-tosyl-2,3,9,9a-tetrahydro-1H-indeno[2,1-c]pyridin-4-yl)(phenyl)methanone

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Chemical Property of (9,9-dimethyl-2-tosyl-2,3,9,9a-tetrahydro-1H-indeno[2,1-c]pyridin-4-yl)(phenyl)methanone

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Technology Process of (9,9-dimethyl-2-tosyl-2,3,9,9a-tetrahydro-1H-indeno[2,1-c]pyridin-4-yl)(phenyl)methanone

There total 2 articles about (9,9-dimethyl-2-tosyl-2,3,9,9a-tetrahydro-1H-indeno[2,1-c]pyridin-4-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 915275-13-7
4-methyl-N-(3-methylbut-2-en-1-yl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide

: 100-52-7
benzaldehyde

: 1542560-52-0
(9,9-dimethyl-2-tosyl-2,3,9,9a-tetrahydro-1H-indeno[2,1-c]pyridin-4-yl)(phenyl)methanone

Guidance literature:: With tert.-butylhydroperoxide; Trimethylacetic acid; In acetonitrile; at 120 ℃; for 48h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c3cc48339h

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 132330-44-0
N-prenyl-N-propargyltosylamide

: 1542560-52-0
(9,9-dimethyl-2-tosyl-2,3,9,9a-tetrahydro-1H-indeno[2,1-c]pyridin-4-yl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; isopropylamine / 20 °C

2: Trimethylacetic acid; tert.-butylhydroperoxide / acetonitrile / 48 h / 120 °C / Schlenk technique; Inert atmosphere

With tert.-butylhydroperoxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; isopropylamine; Trimethylacetic acid; In acetonitrile;
DOI:10.1039/c3cc48339h