(5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane

Base Information

Chemical Name:(5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane
CAS No.:189247-56-1
Molecular Formula:C₄₂H₅₀O₂Si₃
Molecular Weight:671.114
Hs Code.:

Synonyms:(5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane

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Chemical Property of (5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane

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Technology Process of (5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane

There total 3 articles about (5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 175982-50-0
C₃₀H₄₀OSi₂

: 189247-56-1
(5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane

: 176198-95-1
(S)-(E)-4-(dimethylphenylsilyl)-2-decene

Guidance literature:: With 1,1,3,3-tetramethylbutane isonitrile; palladium(II) acetylacetonate; In toluene; for 3h; Heating;
DOI:10.1002/chem.200401031

Reference yield:

: 18666-34-7
1-chloro-2,2-dimethyl-1,1,2-triphenyl-disilane

: 189247-56-1
(5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N; 4-dimethylaminopyridine / tetrahydrofuran / 20 °C

2: 46 percent / 1,1,3,3-tetramethylbutyl isocyanide / [Pd(acac)2] / toluene / 3 h / Heating

With dmap; 1,1,3,3-tetramethylbutane isonitrile; triethylamine; palladium(II) acetylacetonate; In tetrahydrofuran; toluene;
DOI:10.1002/chem.200401031

Reference yield:

: (E)-(R)-Dec-3-en-2-ol

: 189247-56-1
(5S,6R)-5-[(S)-1-(Dimethyl-phenyl-silanyl)-heptyl]-6-methyl-2,2,4,4-tetraphenyl-[1,3,2,4]dioxadisilinane

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N; 4-dimethylaminopyridine / tetrahydrofuran / 20 °C

2: 46 percent / 1,1,3,3-tetramethylbutyl isocyanide / [Pd(acac)2] / toluene / 3 h / Heating

With dmap; 1,1,3,3-tetramethylbutane isonitrile; triethylamine; palladium(II) acetylacetonate; In tetrahydrofuran; toluene;
DOI:10.1002/chem.200401031