triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

Base Information

Chemical Name:triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane
CAS No.:1300750-03-1
Molecular Formula:C₃₃H₄₀N₂O₅SSi
Molecular Weight:604.843
Hs Code.:

Synonyms:triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

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Chemical Property of triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

Chemical Property:

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Technology Process of triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

There total 4 articles about triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300749-88-5
(E)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1-en-7-yn-3-one

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1300750-03-1
triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

: triisopropyl[(1E,3E)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201003019

Reference yield:

: C₁₇H₂₀OSi

: 1300750-03-1
triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

: triisopropyl[(1E,3E)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / tetrahydrofuran / Inert atmosphere

2: potassium carbonate / acetonitrile / 6 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With N-Bromosuccinimide; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/chem.201003019

Reference yield:

: 66920-75-0
4-(naphthalen-1-yl)but-3-en-2-one

: 1300750-03-1
triisopropyl[(1E,3Z)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

: triisopropyl[(1E,3E)-1-(naphth-1-yl)-5-(p-nitrobenzenesulfonyl)-5-azanona-1,3-dien-7-yn-3-yloxy]silane

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1.33 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 - 20 °C / Inert atmosphere

2.1: N-Bromosuccinimide / tetrahydrofuran / Inert atmosphere

3.1: potassium carbonate / acetonitrile / 6 h / 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With N-Bromosuccinimide; potassium carbonate; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/chem.201003019