Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)}{BF₄}

Base Information

• Chemical Name: Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)}{BF₄}
• CAS No.: 155806-24-9
• Molecular Formula: BF₄*C₄₉H₄₇IrP₃S
• Molecular Weight: 1039.92

Synonyms:Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)}{BF₄}

Chemical Property of Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)}{BF₄}

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Technology Process of Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)}{BF₄}

There total 1 articles about Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)}{BF₄} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

tetrafluoroboric acid diethyl ether (67969-82-8) + Ir(triphos)(η(3)-2-vinylthiophenolate) (156701-47-2) → Ir(CH3C(CH2P(C6H5)2)3)(SC6H4CHCH3)(1+)*BF4(1-)={Ir(CH3C(CH2P(C6H5)2)3)(SC6H4CHCH3)}{BF4} (155806-24-9)

Guidance literature:

In tetrahydrofuran; under N2; to a soln. of the Ir complex in THF was added a stoich. amt. of HBF4*Et2O at 0°C, after 30 min warmed to room temp.; addn. of heptane; elem. anal.;

DOI:10.1021/ja00089a027

Reference yield: 60.0%

Ir(CH3C(CH2P(C6H5)2)3)(SC6H4CHCH3)(1+)*BF4(1-)={Ir(CH3C(CH2P(C6H5)2)3)(SC6H4CHCH3)}{BF4} (155806-24-9) + lithium triethylborohydride (22560-16-3) → IrH(CH3C(CH2P(C6H5)2)3)(SC6H4CHCH3)

Guidance literature:

In tetrahydrofuran; under N2; to a stirred soln. of LiHBEt3 in THF was added the solid Ir complex at -70°C, after 15 min the mixt. was allowed to reach room temp.; addn. of ethanol, partial evapn. under reduced pressure, filtered, washed with ethanol and pentane; elem. anal.;

DOI:10.1021/ja00089a027

Reference yield:

Ir(CH3C(CH2P(C6H5)2)3)(SC6H4CHCH3)(1+)*BF4(1-)={Ir(CH3C(CH2P(C6H5)2)3)(SC6H4CHCH3)}{BF4} (155806-24-9) → Ir2H2(CH3C(CH2P(C6H5)2)3)2(SC6H4C2H5)2(2+)*2BF4(1-)={Ir2H2(CH3C(CH2P(C6H5)2)3)2(SC6H4C2H5)2}{BF4}2

Guidance literature:

With H₂; In tetrahydrofuran; a soln. of the Ir complex in THF was stirred under H2 (1-5 atm) at room temp. for 3 h; concd. to dryness under vac.;

DOI:10.1021/ja00089a027

upstream raw materials:

tetrafluoroboric acid diethyl ether

Ir(triphos)(η(3)-2-vinylthiophenolate)

Downstream raw materials:

Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)⁽¹⁺⁾*B(C₆H₅)4^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(SC₆H₄CHCH₃)}{B(C₆H₅)4}

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