N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal

Base Information

Chemical Name:N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal
CAS No.:121374-57-0
Molecular Formula:C₁₆H₂₂N₂O₄
Molecular Weight:306.362
Hs Code.:

Synonyms:N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal

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Technology Process of N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal

There total 4 articles about N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 121374-56-9
N-<2-(2'-oxocyclopentyl)ethyl>-p-nitroaniline ethylene ketal

: 74-88-4
methyl iodide

: 121374-57-0
N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 16h; Ambient temperature;
DOI:10.1021/jo00275a034

Reference yield:

: 54154-07-3
9-(2-hydroxyethyl)-1,4-dioxaspiro<4.4>nonane

: 121374-57-0
N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine, diethyl azodicarboxylate (DEAD) / tetrahydrofuran / 48 h / Ambient temperature

2: 85percent hydrazine hydrate / methanol / 16 h / Heating

3: 52 percent / K₂CO₃ / acetonitrile / 24 h / Heating

4: 85 percent / sodium hydride / tetrahydrofuran / 16 h / Ambient temperature

With sodium hydride; potassium carbonate; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/jo00275a034

Reference yield:

: 121374-55-8
2-(2'-oxocyclopentyl)ethylamine ethylene ketal

: 121374-57-0
N-<2-(2'-oxocyclopentyl)ethyl>-N-methyl-p-nitroaniline ethylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / K₂CO₃ / acetonitrile / 24 h / Heating

2: 85 percent / sodium hydride / tetrahydrofuran / 16 h / Ambient temperature

With sodium hydride; potassium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00275a034