Technology Process of C17H23ClFNO3
There total 7 articles about C17H23ClFNO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium acetate;
In
ethanol;
for 7h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / acetone / 20 °C / Inert atmosphere
2: ammonium acetate / ethanol / 7 h / Reflux
With
ammonium acetate; toluene-4-sulfonic acid;
In
ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: n-butyllithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark
3.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.08 h / 0 - 25 °C / Inert atmosphere
3.2: 1 h / Inert atmosphere
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 25 °C
5.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -60 °C / Inert atmosphere
6.1: toluene-4-sulfonic acid / acetone / 20 °C / Inert atmosphere
7.1: ammonium acetate / ethanol / 7 h / Reflux
With
lithium aluminium tetrahydride; n-butyllithium; diethylamino-sulfur trifluoride; ammonium acetate; toluene-4-sulfonic acid; N-cyclohexyl-cyclohexanamine;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; di-isopropyl ether; acetone; toluene;