1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil

Base Information

Chemical Name:1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil
CAS No.:100682-93-7
Molecular Formula:C₂₀H₂₅N₅O₇
Molecular Weight:447.448
Hs Code.:

Synonyms:1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil

Suppliers and Price of 1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil

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Chemical Property of 1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil

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Technology Process of 1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil

There total 9 articles about 1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 100682-99-3
[(S)-1-({(R)-Carbamoyl-[(2R,3S,4R,5R)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-3,4-dihydroxy-tetrahydro-furan-2-yl]-methyl}-methyl-carbamoyl)-2-phenyl-ethyl]-carbamic acid benzyl ester

: 100682-93-7
1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil

Guidance literature:: With formic acid; palladium; In methanol; for 0.5h;
DOI:10.1021/jo00362a027

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 100682-93-7
1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 18 h / 25 °C

2: acetic acid / H₂O / 5 h

3: 77 percent / AG₅₀WX₈(H+) / dioxane; H₂O / 16 h / Heating

4: 70 percent / formic acid / Pd black / methanol / 0.5 h

With formic acid; AG₅₀WX₈(H+); acetic acid; palladium; In 1,4-dioxane; methanol; water;
DOI:10.1021/jo00362a027

Reference yield:

: 34311-30-3
2',3'-O-cyclohexylideneuridine 5'-aldehyde

: 100682-93-7
1-<5'-(L-phenylalanylmethylamino)-5'-deoxy-α-L-talo-furanosyluronic acid amide>uracil

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / 3A sieves / tetrahydrofuran / 2 h / Ambient temperature

2: methanol / 18 h / 25 °C

3: acetic acid / H₂O / 5 h

4: 77 percent / AG₅₀WX₈(H+) / dioxane; H₂O / 16 h / Heating

5: 70 percent / formic acid / Pd black / methanol / 0.5 h

With formic acid; 3 A molecular sieve; AG₅₀WX₈(H+); acetic acid; palladium; In tetrahydrofuran; 1,4-dioxane; methanol; water;
DOI:10.1021/jo00362a027