(6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol

Base Information

Chemical Name:(6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol
CAS No.:125458-53-9
Molecular Formula:C₃₁H₄₈O₃S
Molecular Weight:500.786
Hs Code.:

Synonyms:(6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol

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Chemical Property of (6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol

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Technology Process of (6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol

There total 8 articles about (6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 125458-57-3
Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

: 125458-53-9
(6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol

Guidance literature:: With sodium hydroxide; In methanol; for 24h; Heating;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 125458-53-9
(6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / p-TsOH / CH₂Cl₂ / 4 h / Ambient temperature

2: 94 percent / 2N NaOH / methanol / 24 h / Heating

With sodium hydroxide; toluene-4-sulfonic acid; In methanol; dichloromethane;

Reference yield:

: 31236-13-2,60441-27-2,69538-05-2,69538-06-3,69659-77-4,69659-78-5,74986-29-1
10,11-oxido-E,E-farnesyl phenyl sulfide

: 125458-53-9
(6E,10E,14E)-2,6,10,14-tetramethyl-16-phenylthio-3-tetrahydropyranyloxy-6,10,14-hexadecatrien-4-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / aluminium isopropoxide / toluene / 12 h / Heating

2: 60 percent / 2,4-dinitrophenol / toluene / 1) heated gradually to 125 deg C over 3 h, 2) 125 deg C, 30 h

3: 100 percent / NaBH₄ / methanol / 0.5 h / Ambient temperature

4: 95 percent / p-TsOH / CH₂Cl₂ / 4 h / Ambient temperature

5: 94 percent / 2N NaOH / methanol / 24 h / Heating

With sodium hydroxide; sodium tetrahydroborate; 2,4-Dinitrophenol; aluminum isopropoxide; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;