Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Base Information

Chemical Name:Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester
CAS No.:125458-57-3
Molecular Formula:C₃₈H₅₂O₄S
Molecular Weight:604.894
Hs Code.:

Synonyms:Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

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Chemical Property of Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

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Technology Process of Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

There total 7 articles about Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 125458-52-8
(6E,10E,14E)-3-hydroxy-2,6,10,14-tetramethyl-16-phenylthio-6,10,14-hexadecatrien-4-yl benzoate

: 125458-57-3
Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; for 4h; Ambient temperature;

Reference yield:

: 31236-13-2,60441-27-2,69538-05-2,69538-06-3,69659-77-4,69659-78-5,74986-29-1
10,11-oxido-E,E-farnesyl phenyl sulfide

: 125458-57-3
Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / aluminium isopropoxide / toluene / 12 h / Heating

2: 60 percent / 2,4-dinitrophenol / toluene / 1) heated gradually to 125 deg C over 3 h, 2) 125 deg C, 30 h

3: 100 percent / NaBH₄ / methanol / 0.5 h / Ambient temperature

4: 95 percent / p-TsOH / CH₂Cl₂ / 4 h / Ambient temperature

With sodium tetrahydroborate; 2,4-Dinitrophenol; aluminum isopropoxide; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;

Reference yield:

: 91496-44-5
3-methyl-2-oxybutyl benzoate

: 125458-57-3
Benzoic acid (3E,7E,11E)-3,7,11-trimethyl-1-[2-methyl-1-(tetrahydro-pyran-2-yloxy)-propyl]-13-phenylsulfanyl-trideca-3,7,11-trienyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / p-TsOH / methanol / 13 h / 50 °C

2: 60 percent / 2,4-dinitrophenol / toluene / 1) heated gradually to 125 deg C over 3 h, 2) 125 deg C, 30 h

3: 100 percent / NaBH₄ / methanol / 0.5 h / Ambient temperature

4: 95 percent / p-TsOH / CH₂Cl₂ / 4 h / Ambient temperature

With sodium tetrahydroborate; 2,4-Dinitrophenol; toluene-4-sulfonic acid; In methanol; dichloromethane; toluene;