methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

• Chemical Name: methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside
• CAS No.: 114405-44-6
• Molecular Formula: C₅₆H₄₇NO₁₇
• Molecular Weight: 1005.99

Synonyms:methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside

Chemical Property of methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 3 articles about methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methyl 6-O-acetyl-3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside (111730-29-1) → methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside (114405-44-6)

Guidance literature:

hydrogenchloride; In methanol; chloroform; at 20 ℃; for 17h;

DOI:10.1016/S0040-4020(01)86852-6

Reference yield:

2,3,4,6-tetra-O-benzoyl-α-D-galactopyranosyl bromide (61198-88-7) → methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside (114405-44-6)

Guidance literature:

Multi-step reaction with 2 steps

1: silver triflate / CH₂Cl₂ / -30 - -25 °C

2: 98 percent / HCl / CHCl₃; methanol / 17 h / 20 °C

With silver trifluoromethanesulfonate; hydrogenchloride; In methanol; dichloromethane; chloroform;

DOI:10.1016/S0040-4020(01)86852-6

Reference yield:

methyl 6-O-acetyl-3-O-benzoyl-2-deoxy-4-O-trityl-2-phthalimido-β-D-glucopyranoside (113369-55-4) → methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside (114405-44-6)

Guidance literature:

Multi-step reaction with 2 steps

1: silver triflate / CH₂Cl₂ / -30 - -25 °C

2: 98 percent / HCl / CHCl₃; methanol / 17 h / 20 °C

With silver trifluoromethanesulfonate; hydrogenchloride; In methanol; dichloromethane; chloroform;

DOI:10.1016/S0040-4020(01)86852-6

upstream raw materials:

methyl 6-O-acetyl-3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-β-D-glucopyranoside

2,3,4,6-tetra-O-benzoyl-α-D-galactopyranosyl bromide

methyl 6-O-acetyl-3-O-benzoyl-2-deoxy-4-O-trityl-2-phthalimido-β-D-glucopyranoside

Downstream raw materials:

methyl 3-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-6-O-trityl-β-D-glucopyranoside

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