[1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester

Base Information

Chemical Name:[1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester
CAS No.:798563-32-3
Molecular Formula:C₂₇H₃₄N₂O₅
Molecular Weight:466.577
Hs Code.:

Synonyms:[1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester

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Chemical Property of [1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester

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Technology Process of [1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester

There total 10 articles about [1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 798563-45-8
1-(3-isopropoxybenzyl)-4-chloromethyl-6,7-dimethoxyisoquinoline

: 798563-32-3
[1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / dimethyl sulfoxide / 1 h / 65 °C

2: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 1 h / 2068.65 Torr

With sodium azide; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; dimethyl sulfoxide;

Reference yield:

: 798563-22-1
1-(3-isopropoxybenzyl)-6,7-dimethoxyisoquinoline-4-methanol

: 798563-32-3
[1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.33 h / 0 °C

1.2: 20 °C

2.1: sodium azide / dimethyl sulfoxide / 1 h / 65 °C

3.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 1 h / 2068.65 Torr

With sodium azide; hydrogen; methanesulfonyl chloride; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1344688-69-2
C₂₄H₃₁NO₆

: 798563-32-3
[1-(3-isopropoxy)benzyl-6,7-di-methoxyi-soquinoline-4-ylmethyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: phosphorus pentachloride / dichloromethane / 0 - 20 °C

2.1: sulfur / 0.33 h / 165 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Heating / reflux

4.1: methanesulfonyl chloride; triethylamine / dichloromethane / 0.33 h / 0 °C

4.2: 20 °C

5.1: sodium azide / dimethyl sulfoxide / 1 h / 65 °C

6.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 1 h / 2068.65 Torr

With lithium aluminium tetrahydride; sodium azide; phosphorus pentachloride; hydrogen; sulfur; methanesulfonyl chloride; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;