3,6-di-tert-butyl-9-(4-methoxycarbonylphenyl)-9H-carbazole

Base Information

Chemical Name:3,6-di-tert-butyl-9-(4-methoxycarbonylphenyl)-9H-carbazole
CAS No.:1219807-24-5
Molecular Formula:C₂₈H₃₁NO₂
Molecular Weight:413.56
Hs Code.:

Synonyms:3,6-di-tert-butyl-9-(4-methoxycarbonylphenyl)-9H-carbazole

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Chemical Property of 3,6-di-tert-butyl-9-(4-methoxycarbonylphenyl)-9H-carbazole

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Technology Process of 3,6-di-tert-butyl-9-(4-methoxycarbonylphenyl)-9H-carbazole

There total 2 articles about 3,6-di-tert-butyl-9-(4-methoxycarbonylphenyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 37500-95-1
3,6-di(tert-butyl)-9H-carbazole

: 619-44-3
methyl 4-iodobenzoate

: 1219807-24-5
3,6-di-tert-butyl-9-(4-methoxycarbonylphenyl)-9H-carbazole

Guidance literature:: With copper(I) oxide; In N,N-dimethyl acetamide; at 160 ℃; for 24h; Inert atmosphere;
DOI:10.1039/b918986f

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 1219807-24-5
3,6-di-tert-butyl-9-(4-methoxycarbonylphenyl)-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 9 h / 0 - 20 °C

2: copper(I) oxide / N,N-dimethyl acetamide / 24 h

With copper(I) oxide; aluminum (III) chloride; In dichloromethane; N,N-dimethyl acetamide; 2: |Ullmann Condensation;
DOI:10.1134/S1070363215060122