(Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride

Base Information

Chemical Name:(Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride
CAS No.:1351238-54-4
Molecular Formula:C₁₄H₉ClN₄O₂S
Molecular Weight:332.77
Hs Code.:

Synonyms:(Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride

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Chemical Property of (Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride

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Technology Process of (Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride

There total 3 articles about (Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1351238-51-1
N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carboxamide

: 1351238-54-4
(Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride

Guidance literature:: With trichlorophosphate; at 105 ℃; for 7h;

Reference yield:

: 99-55-8
2-methyl-5-nitroaniline

: 1351238-54-4
(Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.25 h

1.2: 60 h / 60 °C

2.1: trichlorophosphate / 7 h / 105 °C

With N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate; In N,N-dimethyl-formamide;

Reference yield:

: 59944-79-5
thieno[2,3-b]pyrazine-6-carboxylic acid

: 1351238-54-4
(Z)-N-(2-methyl-5-nitrophenyl)thieno[2,3-b]pyrazine-6-carbimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.25 h

1.2: 60 h / 60 °C

2.1: trichlorophosphate / 7 h / 105 °C

With N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate; In N,N-dimethyl-formamide;