2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol

Base Information

Chemical Name:2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol
CAS No.:87059-28-7
Molecular Formula:C₂₇H₃₆N₂O₅Se₂
Molecular Weight:626.513
Hs Code.:

Synonyms:2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol

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Chemical Property of 2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol

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Technology Process of 2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol

There total 9 articles about 2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 51694-22-5
ortho-nitrophenyl selenocyanate

: 87059-26-5
(S)-2-[(1S,2S,5R)-2-(2-Hydroxy-ethyl)-5-(1-hydroxy-1-methyl-ethyl)-2-methyl-cyclohexyl]-propan-1-ol

: 87059-28-7
2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol

Guidance literature:: With tributylphosphine; In tetrahydrofuran; pyridine; for 18h; Ambient temperature;

Reference yield:

: 83093-41-8,83093-45-2
(S)-7-(1,2-Dihydroxy-1-methyl-ethyl)-1,4a-dimethyl-4,4a,5,6-tetrahydro-3H-naphthalen-2-one

: 87059-28-7
2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol

Guidance literature:: Multi-step reaction with 9 steps

1: 24 percent / potassium hydroxide, H₂ / 10percent palladium charcoal / ethanol / 0.5 h / 760 Torr / Ambient temperature

2: 91 percent / pyridine / 44 h / Ambient temperature

3: 97 percent / basic alumina

4: 94 percent / LAH / diethyl ether / 12 h / Heating

5: 92 percent / chromium trioxide / pyridine / 3 h / Ambient temperature

6: 99 percent / boron trifluoride etherate / benzene / 4 h / Ambient temperature

7: 76 percent / etheral methyllithium / tetrahydrofuran / 0.33 h / 0 °C

8: 77 percent / ozone, sodium borohydride / methanol; CH₂Cl₂ / 0.58 h / -77 °C

9: 84 percent / tri-n-butyl phosphine / tetrahydrofuran; pyridine / 18 h / Ambient temperature

With pyridine; chromium(VI) oxide; aluminum oxide; potassium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; tributylphosphine; boron trifluoride diethyl etherate; methyllithium; hydrogen; ozone; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; diethyl ether; ethanol; dichloromethane; benzene;

Reference yield:

: 87059-23-2,87059-30-1
Toluene-4-sulfonic acid 2-((2R,4aS,8aS)-4a,8-dimethyl-7-oxo-decahydro-naphthalen-2-yl)-2-hydroxy-propyl ester

: 87059-28-7
2-{(1R,3S,4S)-4-Methyl-3-[(S)-1-methyl-2-(2-nitro-phenylselanyl)-ethyl]-4-[2-(2-nitro-phenylselanyl)-ethyl]-cyclohexyl}-propan-2-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 97 percent / basic alumina

2: 94 percent / LAH / diethyl ether / 12 h / Heating

3: 92 percent / chromium trioxide / pyridine / 3 h / Ambient temperature

4: 99 percent / boron trifluoride etherate / benzene / 4 h / Ambient temperature

5: 76 percent / etheral methyllithium / tetrahydrofuran / 0.33 h / 0 °C

6: 77 percent / ozone, sodium borohydride / methanol; CH₂Cl₂ / 0.58 h / -77 °C

7: 84 percent / tri-n-butyl phosphine / tetrahydrofuran; pyridine / 18 h / Ambient temperature

With chromium(VI) oxide; aluminum oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; tributylphosphine; boron trifluoride diethyl etherate; methyllithium; ozone; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; benzene;