Technology Process of trans-Dihydrocarisson-tosylhydrazon
There total 7 articles about trans-Dihydrocarisson-tosylhydrazon which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
benzene;
for 4h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 24 percent / potassium hydroxide, H2 / 10percent palladium charcoal / ethanol / 0.5 h / 760 Torr / Ambient temperature
2: 91 percent / pyridine / 44 h / Ambient temperature
3: 97 percent / basic alumina
4: 94 percent / LAH / diethyl ether / 12 h / Heating
5: 92 percent / chromium trioxide / pyridine / 3 h / Ambient temperature
6: 99 percent / boron trifluoride etherate / benzene / 4 h / Ambient temperature
With
pyridine; chromium(VI) oxide; aluminum oxide; potassium hydroxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; hydrogen;
palladium on activated charcoal;
In
pyridine; diethyl ether; ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 97 percent / basic alumina
2: 94 percent / LAH / diethyl ether / 12 h / Heating
3: 92 percent / chromium trioxide / pyridine / 3 h / Ambient temperature
4: 99 percent / boron trifluoride etherate / benzene / 4 h / Ambient temperature
With
chromium(VI) oxide; aluminum oxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate;
In
pyridine; diethyl ether; benzene;
