(S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate

Base Information

Chemical Name:(S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate
CAS No.:1264263-57-1
Molecular Formula:C₂₁H₂₃N₃O₆
Molecular Weight:413.43
Hs Code.:

Synonyms:(S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate

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Chemical Property of (S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate

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Technology Process of (S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate

There total 9 articles about (S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1264243-55-1
5-acetoxynicotinoyl chloride

: 1264239-65-7
(S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride

: 1264263-57-1
(S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate

Guidance literature:: 5-acetoxynicotinoyl chloride; (S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride; With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 18h;

With 1-amino-3-(dimethylamino)propane; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield: 81.0%

: 1264263-56-0
C₂₃H₂₅N₃O₇

: 1264263-57-1
(S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate

Guidance literature:: With 1-amino-3-(dimethylamino)propane; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 27828-71-3
5-hydroxynicotinic acid

: 1264263-57-1
(S)-allyl 2-(benzyloxycarbonylamino)-3-(5-hydroxy-N-methylnicotinamido)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 0.75 h / 95 °C

2.1: N,N-dimethyl-formamide; oxalyl dichloride / chloroform / 15 h / 20 °C

3.1: triethylamine / tetrahydrofuran / 18 h / 0 - 20 °C

3.2: 2 h / 20 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; chloroform;