(S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride

Base Information

Chemical Name:(S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride
CAS No.:1264239-65-7
Molecular Formula:C₁₅H₂₀N₂O₄*ClH
Molecular Weight:328.796
Hs Code.:

Synonyms:(S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride

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Chemical Property of (S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride

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Technology Process of (S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride

There total 4 articles about (S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 107-18-6
allyl alcohol

: Z-Dap(Me)-OH hydrochloride

: 1264239-65-7
(S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride

Guidance literature:: allyl alcohol; Z-Dap(Me)-OH hydrochloride; With thionyl chloride; at 20 - 70 ℃; for 1.75h;

With sodium hydrogencarbonate; In dichloromethane; water;

With hydrogenchloride; In 1,4-dioxane; dichloromethane; water; for 0.0833333h;

Reference yield:

: C₂₁H₂₃N₃O₈S

: 1264239-65-7
(S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride

Guidance literature:: C₂₁H₂₃N₃O₈S; With potassium carbonate; thiophenol; In acetonitrile; at 0 - 10 ℃; for 2.5h;

With hydrogenchloride; In 1,4-dioxane; dichloromethane;

Reference yield:

: 1145-80-8
N-(benzyloxycarbonyl)-L-serine

: 1264239-65-7
(S)-allyl 2-(benzyloxycarbonylamino)-3-(methylamino)propanoate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; diethylazodicarboxylate

2.1: thionyl chloride / 1.75 h / 20 - 70 °C

2.2: 0.08 h

With thionyl chloride; triphenylphosphine; diethylazodicarboxylate;