3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester

Base Information

Chemical Name:3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester
CAS No.:107688-37-9
Molecular Formula:C₂₉H₃₆N₂O₇S
Molecular Weight:556.68
Hs Code.:

Synonyms:3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester

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Chemical Property of 3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester

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Technology Process of 3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester

There total 14 articles about 3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107704-41-6
3-Benzyloxycarbonyl-5-(3-hydroxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuemethylester

: 124-63-0
methanesulfonyl chloride

: 107688-37-9
3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester

Guidance literature:: With triethylamine; In dichloromethane; for 0.25h;
DOI:10.1016/S0040-4020(01)86686-2

Reference yield:

: 107704-36-9
3-Benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-ol

: 107688-37-9
3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 7 steps

1: acetylation

3: H₂O₂, OH^-

4: Amberlyst 15

5: H₂ / Pd/C

7: Et₃N

With Amberlyst 15; hydroxide; hydrogen; dihydrogen peroxide; triethylamine; palladium on activated charcoal;
DOI:10.1002/hlca.19860690225

Reference yield:

: 107704-37-0
8-Acetoxy-3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol

: 107688-37-9
3-Benzyloxycarbonyl-5-(3-methansulfonoxypropyl)-1,2,4,5,6,7,8,9-octahydro-3H-azecino<5,4-b>indol-8-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 6 steps

2: H₂O₂, OH^-

3: Amberlyst 15

4: H₂ / Pd/C

6: Et₃N

With Amberlyst 15; hydroxide; hydrogen; dihydrogen peroxide; triethylamine; palladium on activated charcoal;
DOI:10.1002/hlca.19860690225