dimethyl heptalene-4,5-dicarboxylate

Base Information

Chemical Name:dimethyl heptalene-4,5-dicarboxylate
CAS No.:58150-88-2
Molecular Formula:C₁₆H₁₄O₄
Molecular Weight:270.285
Hs Code.:

Synonyms:dimethyl heptalene-4,5-dicarboxylate

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Chemical Property of dimethyl heptalene-4,5-dicarboxylate

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Technology Process of dimethyl heptalene-4,5-dicarboxylate

There total 1 articles about dimethyl heptalene-4,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58150-95-1
(1S,3aR)-1H-1,3a-Etheno-azulene-9,10-dicarboxylic acid dimethyl ester

: 58150-88-2
dimethyl heptalene-4,5-dicarboxylate

: 762-42-5
dimethyl acetylenedicarboxylate

: 275-51-4
azulene

Guidance literature:: In ⁽²⁾H₈-toluene; at 60 ℃; for 30h; under 750.06 Torr; thermolyse, other pressure;

Reference yield: 69.0%

: 3112-85-4
methylphenylsulfonate

: 58150-88-2
dimethyl heptalene-4,5-dicarboxylate

: dimethyl (3R*,4R*)-3,4-dihydro-3-[(phenylsulfonyl)methyl]heptalene-4,5-dicarboxylate

Guidance literature:: methylphenylsulfonate; With n-butyllithium; In tetrahydrofuran; hexane; at -10 - 0 ℃; Inert atmosphere;

dimethyl heptalene-4,5-dicarboxylate; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1002/hlca.201100510

Reference yield: 67.0%

: 58150-88-2
dimethyl heptalene-4,5-dicarboxylate

: 599-70-2
ethyl phenyl sulfone

: dimethyl (1'S*,3R*,4R*)-3,4-dihydro-3-[(1-phenylsulfonyl)ethyl]heptalene-4,5-dicarboxylate

Guidance literature:: ethyl phenyl sulfone; With n-butyllithium; In tetrahydrofuran; hexane; at -10 - 0 ℃; Inert atmosphere;

dimethyl heptalene-4,5-dicarboxylate; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1002/hlca.201100510